7FF8
Pseudomonas aeruginosa Virulence Factor Regulator with cAMP ligand and Cl(triethylphosphine)gold(I)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 05A |
Synchrotron site | NSRRC |
Beamline | TPS 05A |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2019-08-07 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.04 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 140.264, 49.928, 62.381 |
Unit cell angles | 90.00, 100.14, 90.00 |
Refinement procedure
Resolution | 34.520 - 2.800 |
R-factor | 0.2721 |
Rwork | 0.269 |
R-free | 0.32650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2oz6 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.353 |
Data reduction software | HKL-3000 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.300 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 21209 | 2078 |
<I/σ(I)> | 13.46 | |
Completeness [%] | 99.9 | |
Redundancy | 2 | |
CC(1/2) | 0.975 | 0.351 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 2.6M Ammonium Sulphate, 0.1M Bicine |