7F9F
Thrombocorticin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-22 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.97892 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.458, 92.445, 58.536 |
Unit cell angles | 90.00, 102.76, 90.00 |
Refinement procedure
Resolution | 30.474 - 1.411 |
R-factor | 0.17 |
Rwork | 0.169 |
R-free | 0.19370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7f91 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.882 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.430 |
High resolution limit [Å] | 1.410 | 1.410 |
Number of reflections | 84334 | 4206 |
<I/σ(I)> | 25.2 | |
Completeness [%] | 99.9 | |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | MgCl2, Tris, PEG 4000 |