Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 123.15 |
| Detector technology | CCD |
| Collection date | 2014-12-28 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9792 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 308.956, 106.663, 198.708 |
| Unit cell angles | 90.00, 125.96, 90.00 |
Refinement procedure
| Resolution | 33.877 - 3.366 |
| R-factor | 0.2579 |
| Rwork | 0.256 |
| R-free | 0.29390 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2r5k |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.420 |
| High resolution limit [Å] | 3.360 | 3.360 |
| Number of reflections | 70378 | 6595 |
| <I/σ(I)> | 10.8 | |
| Completeness [%] | 95.2 | |
| Redundancy | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.1M Succinic acid pH 5.5, 9.5% PEG 3350 |
