7F74
Rv3094c in complex with FMN.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 289.15 |
Detector technology | CCD |
Collection date | 2019-06-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 172.058, 134.223, 109.411 |
Unit cell angles | 90.00, 128.93, 90.00 |
Refinement procedure
Resolution | 42.550 - 2.000 |
R-factor | 0.192 |
Rwork | 0.190 |
R-free | 0.23270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4kcf |
Data scaling software | Aimless |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.550 | 2.071 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 123413 | 12343 |
<I/σ(I)> | 9.19 | |
Completeness [%] | 94.5 | |
Redundancy | 1.9 | |
CC(1/2) | 0.995 | 0.929 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 289.15 | 0.2M sodium nitrate, 0.1M Bis Tris propane pH=8.5, 20% w/v PEG3350 |