7F25

Crystal structure of SSB from Salmonella enterica serovar Typhimurium LT2.

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13C1
Synchrotron site	NSRRC
Beamline	BL13C1
Temperature [K]	298
Detector technology	CCD
Collection date	2017-10-06
Detector	ADSC QUANTUM 210
Wavelength(s)	0.975
Spacegroup name	P 32 2 1
Unit cell lengths	91.888, 91.888, 61.048
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	28.500 - 2.870
R-factor	0.2361
Rwork	0.233
R-free	0.29580
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1eyg
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX (1.19.1_4122)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.970
High resolution limit [Å]	2.870	2.870
Number of reflections	7050	691
<I/σ(I)>	20.34	2.31
Completeness [%]	99.9	99.7
Redundancy	5.3	4.9
CC(1/2)	0.792	0.918

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	298	15% PEG 400, 100mM sodium Salt, pH6.5