7EPU
Crystal structure of HsALC1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 277 |
Detector technology | PIXEL |
Collection date | 2019-10-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 153.480, 225.263, 106.533 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.560 |
High resolution limit [Å] | 3.500 | 9.480 | 3.500 |
Rmerge | 0.130 | 0.034 | 1.497 |
Rmeas | 0.137 | 0.036 | 1.583 |
Rpim | 0.042 | 0.012 | 0.500 |
Total number of observations | 255064 | ||
Number of reflections | 23523 | 1282 | 1149 |
<I/σ(I)> | 5.5 | ||
Completeness [%] | 99.4 | 99.5 | 97.5 |
Redundancy | 10.8 | 9.4 | 9.9 |
CC(1/2) | 0.999 | 0.514 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | MPD, sodium chloride, magnesium chloride, acetate |