7EHS
Levansucrase from Brenneria sp. EniD 312
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-07 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 98.314, 98.314, 216.475 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 85.140 - 1.600 |
R-factor | 0.1584 |
Rwork | 0.157 |
R-free | 0.18090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4d47 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.725 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 85.150 | 1.390 |
High resolution limit [Å] | 1.340 | 1.340 |
Rpim | 0.025 | 0.456 |
Number of reflections | 80004 | 14170 |
<I/σ(I)> | 17.4 | |
Completeness [%] | 94.6 | 82.3 |
Redundancy | 39 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | Ammonium sulfate, PEG 400 |