7DPD
Human MCM9 N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-06 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.286, 85.900, 111.511 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.110 - 2.550 |
R-factor | 0.2128 |
Rwork | 0.208 |
R-free | 0.26440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Rossetta predicted model |
RMSD bond length | 0.003 |
RMSD bond angle | 0.498 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (dev_3139) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmeas | 0.183 | 0.821 |
Rpim | 0.075 | 0.382 |
Number of reflections | 25165 | 1250 |
<I/σ(I)> | 9.62 | 2.22 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 5.6 | 4.4 |
CC(1/2) | 0.987 | 0.806 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.1M Li2SO4, 0.1M ADA pH 6.2-6.5, 13-16% (w/v) PEG 4000 |