7DNN

Crystal structure of the AgCarB2-C2 complex with homoorientin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron site	Photon Factory
Beamline	AR-NE3A
Temperature [K]	95
Detector technology	PIXEL
Collection date	2019-12-06
Detector	DECTRIS PILATUS 2M-F
Wavelength(s)	1.0000
Spacegroup name	P 21 21 2
Unit cell lengths	73.905, 102.511, 136.090
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.170 - 2.250
R-factor	0.1989
Rwork	0.196
R-free	0.24710
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	0.935
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	CRANK2
Refinement software	PHENIX (1.18_3845)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.970	2.370
High resolution limit [Å]	2.250	2.250
Rmerge	0.054	0.852
Number of reflections	94668	13699
<I/σ(I)>	17.49
Completeness [%]	99.8
Redundancy	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	25%(w/v) PEG4000, 0.1 M MES pH 6.5, 0.2 M Potassium Iodide