7DK8
Crystal structure of OsGH3-8 with AMP
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-13 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.979183 |
Spacegroup name | P 63 |
Unit cell lengths | 121.050, 121.050, 62.670 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.578 - 1.990 |
R-factor | 0.2 |
Rwork | 0.197 |
R-free | 0.25560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4b2g |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.15_3459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.520 | 2.040 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.022 | 0.307 |
Number of reflections | 35491 | 36047 |
<I/σ(I)> | 20.3 | |
Completeness [%] | 98.4 | |
Redundancy | 19.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.08M Tris pH 8.0, 0.1M Tris-HCl (pH 8.5), 22.4% (w/v) PEG 4000, 0.02M Bis-Tris pH 6.5, 5% (w/v) PEG 3350, 0.2 Microliter 275.0mM 2,6-Dimethyl-4-heptyl-beta-D-maltopyranoside |