7DHP
Crystal structure of MazF from Deinococcus radiodurans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2015-12-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 70.490, 70.490, 111.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.830 - 1.300 |
R-factor | 0.1723 |
Rwork | 0.172 |
R-free | 0.18480 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6kys |
RMSD bond length | 0.018 |
RMSD bond angle | 1.652 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 1.340 |
High resolution limit [Å] | 1.300 | 5.830 | 1.300 |
Rmerge | 0.059 | 0.037 | 0.516 |
Rmeas | 0.068 | 0.045 | 0.590 |
Number of reflections | 66360 | 338 | 4953 |
<I/σ(I)> | 14.38 | 21.98 | 3.52 |
Completeness [%] | 96.1 | 37.5 | 99 |
Redundancy | 4.179 | 2.817 | 4.21 |
CC(1/2) | 0.998 | 0.996 | 0.887 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | ammonium sulfate, BIS-TRIS, PEG 3350 |