7D0E
Crystal structure of FIP200 Claw/p-CCPG1 FIR2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-12 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97876 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 51.438, 51.438, 86.151 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.070 - 1.400 |
Rwork | 0.187 |
R-free | 0.20680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6dce |
RMSD bond length | 0.016 |
RMSD bond angle | 1.481 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.037 | |
Rpim | 0.174 | |
Number of reflections | 23548 | 1143 |
<I/σ(I)> | 98.9 | |
Completeness [%] | 99.8 | |
Redundancy | 25.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | KCl, Pentaerythritol ethoxylate (15/4 EO/OH), MES |