7CYB
Saimiri boliviensis boliviensis galectin-13 with glycerol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 33.407, 58.913, 40.701 |
Unit cell angles | 90.00, 113.34, 90.00 |
Refinement procedure
Resolution | 19.820 - 1.600 |
R-factor | 0.1571 |
Rwork | 0.154 |
R-free | 0.18410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6kjx |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.820 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.034 | 0.099 |
Number of reflections | 18965 | 929 |
<I/σ(I)> | 19.5 | |
Completeness [%] | 98.9 | |
Redundancy | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG |