7C0Q

a Legionella pneumophila effector Lpg2505

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	233
Detector technology	PIXEL
Collection date	2018-12-30
Detector	DECTRIS PILATUS3 R CdTe 300K
Wavelength(s)	0.9792
Spacegroup name	P 1 21 1
Unit cell lengths	106.542, 50.448, 122.029
Unit cell angles	90.00, 109.06, 90.00

Refinement procedure

Resolution	92.236 - 2.600
R-factor	0.2309
Rwork	0.229
R-free	0.27550
Structure solution method	SAD
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	92.236	2.640
High resolution limit [Å]	2.600	2.600
Number of reflections	35768	37795
<I/σ(I)>	14.227
Completeness [%]	98.2	99.2
Redundancy	6.9	7.2
CC(1/2)	0.995	0.721

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	0.1 M HEPES pH 7.5, 25% PEG 3350