7BV0
HEV-C E2s
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | PAL-XFEL BEAMLINE NCI |
Synchrotron site | PAL-XFEL |
Beamline | NCI |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2019-10-09 |
Detector | Nonius Kappa CCD |
Wavelength(s) | 0.988 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 107.660, 107.660, 75.458 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.618 - 1.801 |
R-factor | 0.1718 |
Rwork | 0.171 |
R-free | 0.18810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ggq |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.618 | 1.874 |
High resolution limit [Å] | 1.801 | 1.801 |
Number of reflections | 24297 | 24297 |
<I/σ(I)> | 1 | |
Completeness [%] | 99.7 | 99 |
Redundancy | 20 | |
CC(1/2) | 0.750 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293.5 | 0.1 M sodium acetate trihydrate pH 4.5, 3.0 M sodium chloride |