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7B9P

Structure of Ribonucleotide reductase from Rhodobacter sphaeroides

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.1
Synchrotron siteBESSY
Beamline14.1
Temperature [K]100
Detector technologyPIXEL
Collection date2019-01-26
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.9184
Spacegroup nameP 65 2 2
Unit cell lengths140.748, 140.748, 364.277
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution47.860 - 2.646
R-factor0.2312
Rwork0.230
R-free0.27180
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)ensemble
Data reduction softwareXDS
Refinement softwarePHENIX (1.16)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]47.8602.740
High resolution limit [Å]2.6462.650
Rmerge0.1697.684
Rmeas0.1747.886
Rpim0.0401.756
Number of reflections629496078
<I/σ(I)>13.90.3
Completeness [%]99.898.4
Redundancy19.2919.7
CC(1/2)0.9990.148
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8291Precipitant: 30% PEG 1500, 20% Glycerol Protein solution: 45 mg/mL Protein + 100 uM dATP Hanging drop experiment: 1.0 uL Protein solution + 1.0 uL Precipitant over 500 uL precipitant

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