7AH2
Crystal structure of Zebrafish MDM2 RING domain homodimer
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-30 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.163, 23.859, 54.306 |
Unit cell angles | 90.00, 101.66, 90.00 |
Refinement procedure
Resolution | 45.210 - 2.872 |
Rwork | 0.206 |
R-free | 0.28110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vjf |
RMSD bond length | 0.006 |
RMSD bond angle | 1.429 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.185 | 2.922 |
High resolution limit [Å] | 2.872 | 2.872 |
Number of reflections | 2814 | 129 |
<I/σ(I)> | 6.3 | |
Completeness [%] | 100.0 | |
Redundancy | 3.2 | |
CC(1/2) | 0.949 | 0.667 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 292 | 0.1 M imidazole, 0.12 M monosaccharides, 37.5 % (w/v) MPD_P1K_P3350 (Morpheus, Molecular Dimensions) |