7A9C

Human serum albumin (HSA) crystallized in the presence of yttrium (III) chloride

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2009-12-04
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.7
Spacegroup name	P 21 21 21
Unit cell lengths	55.270, 71.930, 180.130
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.002 - 2.750
Rwork	0.238
R-free	0.29460
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2bxi
RMSD bond length	0.002
RMSD bond angle	1.203
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.8.0232 2018/13/08)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	2.820
High resolution limit [Å]	2.750	2.750
Number of reflections	35814	2442
<I/σ(I)>	16.8
Completeness [%]	99.5	93.8
Redundancy	16.2
CC(1/2)	0.999	0.641

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE		293	2mM yttrium chloride