7A8A
rsGreen0.7-K206A-F145Q partially in the green-off state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-28 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9801 |
Spacegroup name | H 3 2 |
Unit cell lengths | 140.760, 140.760, 73.264 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.856 - 1.930 |
R-factor | 0.2062 |
Rwork | 0.204 |
R-free | 0.25380 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.909 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER (2.7.16) |
Refinement software | PHENIX (1.11) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.860 | 46.860 | 1.980 |
High resolution limit [Å] | 1.930 | 9.050 | 1.930 |
Rmerge | 0.052 | 0.035 | 0.670 |
Rmeas | 0.053 | 0.036 | 0.690 |
Rpim | 0.012 | 0.009 | 0.162 |
Total number of observations | 419528 | 3743 | 25718 |
Number of reflections | 20970 | 230 | 1407 |
<I/σ(I)> | 34.1 | 82.3 | 5 |
Completeness [%] | 100.0 | 99.3 | 100 |
Redundancy | 20 | 16.3 | 18.3 |
CC(1/2) | 1.000 | 0.998 | 0.971 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 200 mM NaCl 100 mM MES pH 6.0 20 % PEG 6000 |