7A7P
rsGreen0.7-K206A partially in the green-off state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-28 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9801 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 50.808, 61.352, 65.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.930 - 1.480 |
R-factor | 0.1711 |
Rwork | 0.170 |
R-free | 0.19730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.885 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER (2.7.16) |
Refinement software | PHENIX (1.11) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.930 | 44.930 | 1.510 |
High resolution limit [Å] | 1.480 | 8.110 | 1.480 |
Rmerge | 0.059 | 0.043 | 0.689 |
Rmeas | 0.064 | 0.049 | 0.747 |
Rpim | 0.025 | 0.022 | 0.283 |
Total number of observations | 240614 | ||
Number of reflections | 35063 | 259 | 1716 |
<I/σ(I)> | 15.1 | ||
Completeness [%] | 99.8 | 97.8 | 100 |
Redundancy | 6.9 | 4.7 | 7.1 |
CC(1/2) | 0.998 | 0.994 | 0.876 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 22 % PEG 4000 140 mM Mg(NO3)2 |