Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-06-11 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 153.421, 123.171, 73.126 |
| Unit cell angles | 90.00, 107.90, 90.00 |
Refinement procedure
| Resolution | 47.070 - 2.930 |
| R-factor | 0.2468 |
| Rwork | 0.244 |
| R-free | 0.29010 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3q0x |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.902 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.15_3459) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.080 | 3.110 |
| High resolution limit [Å] | 2.930 | 2.930 |
| Rmeas | 0.011 | |
| Number of reflections | 53262 | 8421 |
| <I/σ(I)> | 9.15 | |
| Completeness [%] | 97.5 | |
| Redundancy | 2.1 | |
| CC(1/2) | 0.410 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 15% PEG 4000, 0.8M sodium formate, 0.1 M Tris pH 8.5 |
