6ZWF
Neisseria gonorrhoeae transaldolase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2020-03-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.7293 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.087, 82.910, 89.465 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.455 - 1.050 |
R-factor | 0.1337 |
Rwork | 0.133 |
R-free | 0.15320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3clm |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.455 | 1.100 |
High resolution limit [Å] | 1.050 | 1.050 |
Rmeas | 0.074 | 1.980 |
Number of reflections | 145716 | 18762 |
<I/σ(I)> | 10.91 | 1.04 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 4.5 | 4.5 |
CC(1/2) | 0.999 | 0.506 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | PEG8000, Citrate, Sodium phosphate, Sodium chloride, Glycylglycin |