6ZUS
Crystal structure of the effector Ecp11-1 from Fulvia fulva
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-25 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9734 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.640, 53.640, 86.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.550 - 1.620 |
R-factor | 0.1848 |
Rwork | 0.184 |
R-free | 0.19670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6zuq |
RMSD bond length | 0.014 |
RMSD bond angle | 1.807 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.550 | 1.720 |
High resolution limit [Å] | 1.620 | 1.620 |
Rmeas | 0.102 | 0.142 |
Number of reflections | 46421 | 7420 |
<I/σ(I)> | 10.56 | 0.86 |
Completeness [%] | 99.7 | |
Redundancy | 7 | |
CC(1/2) | 0.998 | 0.604 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | 21% PEG550MME, 10mM Zinc sulfate, 0.1 MES pH6.5, 15% glycerol |