6ZUQ
Crystal structure of the effector Ecp11-1 from Fulvia fulva
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-12 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.28194 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.760, 53.630, 86.270 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.130 - 1.940 |
R-factor | 0.2007 |
Rwork | 0.200 |
R-free | 0.21210 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.816 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | CRANK2 (2.0.203) |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 43.133 | 43.133 | 2.060 |
High resolution limit [Å] | 1.940 | 5.770 | 1.940 |
Rmerge | 0.112 | 0.055 | 1.319 |
Rmeas | 0.121 | 0.059 | 1.435 |
Total number of observations | 184783 | ||
Number of reflections | 26981 | 1023 | 4248 |
<I/σ(I)> | 10.24 | 31.45 | 1.13 |
Completeness [%] | 99.5 | 99.9 | 97.1 |
Redundancy | 6.849 | 7.334 | 6.407 |
CC(1/2) | 0.997 | 0.999 | 0.413 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 21% PEG550MME, 0.01M zinc sulfate, 0.09M MES pH6.5, 15% glycerol |