6ZT5
Complex between a homodimer of Mycobacterium smegmatis MfpA and a single copy of the N-terminal 47 kDa fragment of the Mycobacterium smegmatis DNA Gyrase B subunit
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-29 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 150.545, 59.380, 141.217 |
Unit cell angles | 90.00, 119.71, 90.00 |
Refinement procedure
Resolution | 75.320 - 2.200 |
R-factor | 0.2102 |
Rwork | 0.208 |
R-free | 0.25150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6zt3 6zt4 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.441 |
Data reduction software | DIALS |
Data scaling software | Aimless (0.7.3) |
Phasing software | PHASER (2.8.2) |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 75.320 | 75.200 | 2.260 |
High resolution limit [Å] | 2.200 | 9.330 | 2.200 |
Rmerge | 0.048 | 0.031 | 1.857 |
Rmeas | 0.052 | 0.035 | 2.022 |
Rpim | 0.020 | 0.014 | 0.787 |
Total number of observations | 5304 | 29306 | |
Number of reflections | 55380 | 795 | 4481 |
<I/σ(I)> | 14.4 | 66.9 | 0.8 |
Completeness [%] | 100.0 | 99.6 | 100 |
Redundancy | 6.9 | 6.7 | 6.5 |
CC(1/2) | 0.996 | 0.991 | 0.608 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | NULL |