6ZS8
X-ray structure of the adduct formed upon treating lysozyme with an aged solution of arsenoplatin-1
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-07-15 |
| Detector | RIGAKU SATURN 944 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 78.703, 78.703, 34.462 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.939 - 2.153 |
| Rwork | 0.185 |
| R-free | 0.23890 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4j1a |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.696 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.650 | 2.190 |
| High resolution limit [Å] | 2.150 | 2.150 |
| Rmerge | 0.113 | 0.639 |
| Number of reflections | 6242 | 301 |
| <I/σ(I)> | 8 | |
| Completeness [%] | 99.5 | 100 |
| Redundancy | 5.7 | 5.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4 | 298 | 20% ethylene glycol 0.1 M sodium acetate pH 4.0 0.6 M sodium nitrate |
