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6ZQ0

Structure of a-l-AraAZI-Bound MgGH51 a-L-Arabinofuranosidase Crystal Type 1

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04-1
Synchrotron siteDiamond
BeamlineI04-1
Temperature [K]100
Detector technologyPIXEL
Collection date2019-12-15
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)0.9119
Spacegroup nameP 21 21 21
Unit cell lengths59.050, 65.460, 191.820
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution61.950 - 1.540
Rwork0.179
R-free0.20580
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6zps
RMSD bond length0.012
RMSD bond angle1.756
Data reduction softwarexia2
Data scaling softwarexia2
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0258)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]61.9501.570
High resolution limit [Å]1.5401.540
Rpim0.0430.731
Number of reflections1109365472
<I/σ(I)>10.60.9
Completeness [%]99.799.7
Redundancy7.76.4
CC(1/2)0.9990.505
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.529310 mg/mL MgGH51 in 10 mM NaOAc, pH 5.5, 100 mM NaCl mixed 2:1 with 20% PEG 3350, 0.1 M Bis-Tris-HCl, pH 6.5, 0.2 M NaNO3

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