6ZPP

g7941: a virulence factor from Drechmaria coniospora

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-01-30
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97918
Spacegroup name	P 1 21 1
Unit cell lengths	44.127, 31.200, 59.316
Unit cell angles	90.00, 91.96, 90.00

Refinement procedure

Resolution	29.640 - 1.500
R-factor	0.1862
Rwork	0.185
R-free	0.20920
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	SCALA (3.3.22)
Phasing software	SHELXDE
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	59.281	29.641	1.580
High resolution limit [Å]	1.500	4.740	1.500
Rmerge		0.115	0.484
Rmeas	0.169	0.151	0.608
Rpim	0.065	0.060	0.234
Total number of observations	175009	5710	24875
Number of reflections	26120	888	3726
<I/σ(I)>	7.4	12.9	2.2
Completeness [%]	99.7	99.3	98.5
Redundancy	6.7	6.4	6.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.05M Na Cacodylate pH5.0-6.0 0.05M Na Acetate 20-30% PEG-5000mme