6ZPN
Crystal structure of Chaetomium thermophilum Raptor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-22 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.999989 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 183.306, 183.306, 271.393 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.610 - 3.500 |
R-factor | 0.2288 |
Rwork | 0.228 |
R-free | 0.24540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ef5 |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18_3845) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.970 | 3.600 |
High resolution limit [Å] | 3.500 | 3.500 |
Number of reflections | 58884 | 4557 |
<I/σ(I)> | 5 | 0.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 12.8 | 13.2 |
CC(1/2) | 0.989 | 0.367 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 303.15 | 0.1 M Bis-Tris pH 5.2-5.3 1.75 M NaCl 12 mM CaCl2 |