6ZNJ
MaeB full-length enzyme apoprotein form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-23 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97951 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 81.705, 273.583, 308.232 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 154.120 | 4.000 |
High resolution limit [Å] | 3.700 | 3.700 |
Number of reflections | 36296 | 1825 |
<I/σ(I)> | 4.6 | 0.5 |
Completeness [%] | 97.1 | |
Redundancy | 13 | |
CC(1/2) | 0.960 | 0.480 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 289 | 0.1M Tris pH 8.0 20% MPD |