6ZN3
Plasmodium facliparum glideosome trimeric sub-complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2020-05-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 43 |
Unit cell lengths | 211.880, 211.880, 75.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.420 | 2.604 |
High resolution limit [Å] | 2.510 | 2.510 |
Rmerge | 0.087 | 3.790 |
Rmeas | 0.095 | 4.118 |
Rpim | 0.037 | 1.602 |
Number of reflections | 114354 | 911 |
<I/σ(I)> | 12.69 | 0.55 |
Completeness [%] | 83.5 | 7.97 |
Redundancy | 6.7 | 6.6 |
CC(1/2) | 0.998 | 0.111 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277.15 | PEG 8000, ethylene glycol, di-ethyleneglycol, tri-ethyleneglycol, tetra-ethyleneglycol, penta-ethyleneglycol, imidazole, MES |