6ZLX

The structure of the ClpX-associated factor PDIP38

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2010-01-20
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1.07
Spacegroup name	P 62
Unit cell lengths	120.095, 120.095, 48.586
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	39.310 - 3.394
R-factor	0.2493
Rwork	0.247
R-free	0.28690
Structure solution method	MAD
RMSD bond length	0.002
RMSD bond angle	0.533
Data reduction software	XDS
Data scaling software	XDS
Phasing software	SHARP
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.310	3.600
High resolution limit [Å]	3.390	3.390
Number of reflections	10813	1742
<I/σ(I)>	15.6
Completeness [%]	99.0
Redundancy	11
CC(1/2)	0.999	0.730

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE		298	20% PEG 8000