6ZBS
Beta ODAP Synthetase (BOS)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2020-06-07 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 66.200, 66.200, 226.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.810 - 2.350 |
R-factor | 0.2089 |
Rwork | 0.206 |
R-free | 0.25940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ke4 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.810 | 2.434 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.100 | 0.688 |
Rpim | 0.165 | 0.272 |
Number of reflections | 21933 | 2130 |
<I/σ(I)> | 49.73 | 5.75 |
Completeness [%] | 98.8 | 99.77 |
Redundancy | 19.3 | |
CC(1/2) | 0.750 | 0.824 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 292 | 0.1M MgCl2 0.05M HEPES pH=7 10% PEG 6000 |