6Z9N
Copper transporter OprC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.35136 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.325, 197.274, 172.119 |
Unit cell angles | 90.00, 91.42, 90.00 |
Refinement procedure
Resolution | 67.300 - 2.730 |
R-factor | 0.2188 |
Rwork | 0.216 |
R-free | 0.26660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fok |
RMSD bond length | 0.009 |
RMSD bond angle | 1.144 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18_3855) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 197.270 | 2.780 |
High resolution limit [Å] | 2.730 | 2.730 |
Rpim | 0.056 | |
Number of reflections | 118817 | 11858 |
<I/σ(I)> | 7.82 | |
Completeness [%] | 100.0 | |
Redundancy | 6.64 | |
CC(1/2) | 0.674 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.34 M Ammonium sulfate 0.1 M Sodium citrate 12 -16 % w/v PEG 4000 2 mM CuSO4 |