6Z99
Copper transporter OprC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-18 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 1.35132 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 154.644, 195.506, 165.629 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 84.180 - 2.680 |
R-factor | 0.2166 |
Rwork | 0.215 |
R-free | 0.25240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fok |
RMSD bond length | 0.009 |
RMSD bond angle | 1.121 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18_3855) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.180 | 2.730 |
High resolution limit [Å] | 2.680 | 2.680 |
Rpim | 0.056 | |
Number of reflections | 70434 | 6894 |
<I/σ(I)> | 0.996 | |
Completeness [%] | 99.9 | |
Redundancy | 13.51 | |
CC(1/2) | 0.575 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.2 M Choline chloride 0.1 M Tris 12-16 % w/v PEG 2000 MME |