Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-05-15 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 0.99999 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 126.960, 126.960, 124.600 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.890 - 2.171 |
| Rwork | 0.214 |
| R-free | 0.24460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6yul |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.420 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.890 | 2.230 |
| High resolution limit [Å] | 2.170 | 2.170 |
| Number of reflections | 54337 | 4362 |
| <I/σ(I)> | 16.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 26.5 | |
| CC(1/2) | 0.999 | 0.761 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M ammonia sulphate 0.1 M bis-tris pH 5.5 23-26% PEG 3350 |
