Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-11 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000031 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 76.186, 212.992, 94.639 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.461 - 3.192 |
Rwork | 0.286 |
R-free | 0.29430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6yvr |
RMSD bond length | 0.002 |
RMSD bond angle | 1.196 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.461 | 3.435 |
High resolution limit [Å] | 3.192 | 3.192 |
Rmerge | 0.330 | 3.661 |
Rmeas | 0.344 | 3.807 |
Rpim | 0.094 | 1.034 |
Number of reflections | 10818 | 541 |
<I/σ(I)> | 7.7 | 1.3 |
Completeness [%] | 91.6 | |
Redundancy | 13.3 | |
CC(1/2) | 0.993 | 0.316 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 4.5 | 293.1 | 100 mM Na acetate 400-475 mM K citrate 30-31% (v/v) PEG400 |