6Z5Y
Structure of a novel LPMO from Phytophthora infestans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | DIAMOND |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-01 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.916 |
Spacegroup name | P 1 |
Unit cell lengths | 36.293, 45.458, 53.687 |
Unit cell angles | 83.91, 71.85, 83.78 |
Refinement procedure
Resolution | 28.790 - 1.010 |
R-factor | 0.1441 |
Rwork | 0.143 |
R-free | 0.16400 |
Structure solution method | AB INITIO PHASING |
RMSD bond length | 0.015 |
RMSD bond angle | 1.957 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | Fragon |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.790 | 28.770 | 1.030 |
High resolution limit [Å] | 1.010 | 5.530 | 1.010 |
Rmerge | 0.048 | 0.035 | 0.680 |
Rmeas | 0.057 | 0.041 | 0.856 |
Rpim | 0.030 | 0.021 | 0.509 |
Number of reflections | 156702 | 992 | 6765 |
<I/σ(I)> | 8.9 | ||
Completeness [%] | 92.4 | 95.9 | 80.9 |
Redundancy | 3.3 | 3.8 | 2.7 |
CC(1/2) | 0.998 | 0.997 | 0.589 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 20mM Tris pH 7.0, 22% Polyethylene Glycol (PEG) 3350 |