6Z4E
The structure of the C-terminal domain of RssB from E. coli
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-05-20 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 56.239, 56.239, 294.462 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.533 - 2.000 |
R-factor | 0.2133 |
Rwork | 0.212 |
R-free | 0.24250 |
Structure solution method | MIR |
RMSD bond length | 0.003 |
RMSD bond angle | 0.630 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.100 | |
Number of reflections | 18222 | 1408 |
<I/σ(I)> | 25.2 | |
Completeness [%] | 91.8 | |
Redundancy | 20 | |
CC(1/2) | 1.000 | 0.850 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 20% PEG1000 |