6Z3B
Low resolution structure of RgNanOx
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2019-04-08 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | I 41 2 2 |
| Unit cell lengths | 150.100, 150.100, 193.310 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 118.560 - 2.580 |
| R-factor | 0.21428 |
| Rwork | 0.212 |
| R-free | 0.24971 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5ui9 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.542 |
| Data reduction software | Aimless |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 119.000 | 2.700 |
| High resolution limit [Å] | 2.580 | 2.580 |
| Number of reflections | 34401 | 1871 |
| <I/σ(I)> | 7.5 | |
| Completeness [%] | 98.6 | |
| Redundancy | 7.5 | |
| CC(1/2) | 1.000 | 1.000 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG3000, sodium citrate |
