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6Z0J

Crystal structure of laccase from Pediococcus acidilactici Pa5930 (Tris-HCl pH 8.5)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALBA BEAMLINE XALOC
Synchrotron siteALBA
BeamlineXALOC
Temperature [K]100
Detector technologyPIXEL
Collection date2018-06-06
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.97925
Spacegroup nameP 21 21 21
Unit cell lengths51.797, 94.294, 97.564
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution67.800 - 2.500
R-factor0.2227
Rwork0.220
R-free0.26790
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3zdw
RMSD bond length0.003
RMSD bond angle1.264
Data reduction softwareXDS
Data scaling softwareAimless (0.2.8)
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0238)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]94.29094.2902.600
High resolution limit [Å]2.5009.0102.500
Rmerge0.1480.0630.904
Rmeas0.1600.0690.970
Rpim0.0580.0270.350
Total number of observations124640264814100
Number of reflections171804371879
<I/σ(I)>7.917.32.2
Completeness [%]100.099.9100
Redundancy7.36.17.5
CC(1/2)0.9950.9950.758
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.529430% PEG1000 and 0.1M Tris-HCl pH 8.5

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