Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 120.790, 120.790, 114.393 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.470 | 3.130 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.089 | 1.079 |
Number of reflections | 10879 | 1704 |
<I/σ(I)> | 12.6 | |
Completeness [%] | 100.0 | |
Redundancy | 9.6 | |
CC(1/2) | 0.998 | 0.917 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 100 mM Sodium citrate, 200 mM Ammonium acetate and 6% MPD |