6YXE
Structure of the Trim69 RING domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-10 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 1.2524 |
Spacegroup name | H 3 2 |
Unit cell lengths | 109.965, 109.965, 90.135 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 65.460 - 2.100 |
R-factor | 0.1999 |
Rwork | 0.198 |
R-free | 0.23950 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.570 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.15) |
Phasing software | SHELXDE |
Refinement software | REFMAC (5.0.32) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 65.460 | 42.100 | 2.160 |
High resolution limit [Å] | 2.100 | 8.910 | 2.100 |
Rmerge | 0.111 | 0.042 | 2.145 |
Rmeas | 0.113 | 0.044 | 2.219 |
Rpim | 0.024 | 0.010 | 0.558 |
Total number of observations | 3484 | 15246 | |
Number of reflections | 12387 | 182 | 999 |
<I/σ(I)> | 27.4 | 107.1 | 1.5 |
Completeness [%] | 100.0 | 99.2 | 100 |
Redundancy | 21.5 | 19.1 | 15.3 |
CC(1/2) | 1.000 | 1.000 | 0.508 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 1.26 M NH4SO4, 0.2 M LiSO4, and 0.1 M Tris pH 8.5 |