6YQF
Crystal structure of the SYCE2-TEX12 delta-Ctip complex in a 4:4 assembly
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-08-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9688 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 42.670, 59.680, 156.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.450 - 3.330 |
R-factor | 0.3286 |
Rwork | 0.327 |
R-free | 0.36720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6r17 |
RMSD bond length | 0.001 |
RMSD bond angle | 0.272 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.452 | 3.594 |
High resolution limit [Å] | 3.327 | 3.327 |
Rmeas | 0.246 | 2.445 |
Rpim | 0.098 | 0.906 |
Number of reflections | 4098 | 342 |
<I/σ(I)> | 4.7 | 1 |
Completeness [%] | 64.8 | 27.1 |
Redundancy | 6.5 | 7.2 |
CC(1/2) | 0.995 | 0.516 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M sodium acetate, 65% MPD |