6YOG
Structure of PepTSt from COC IMISX setup collected by still serial crystallography on crystals prelocated by 2D X-ray phase-contrast imaging
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 102.430, 110.700, 111.280 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.640 - 2.300 |
R-factor | 0.2428 |
Rwork | 0.241 |
R-free | 0.27230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5d58 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHENIX |
Refinement software | PHENIX (dev_3311) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.640 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmeas | 0.170 | 2.150 |
Number of reflections | 28437 | 2806 |
<I/σ(I)> | 3.73 | |
Completeness [%] | 100.0 | 99.95 |
Redundancy | 51.9 | 32.6 |
CC(1/2) | 0.920 | 0.330 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 7 | 293 | 250-325 mM NH4H2PO4, 100 mM HEPES, pH 7.0, 21-22 %(v/v) PEG 400 and 10 mM Ala-Phe |