6YLM
mCherry
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-09 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 1.5419 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 107.280, 42.920, 85.770 |
Unit cell angles | 90.00, 128.50, 90.00 |
Refinement procedure
Resolution | 67.120 - 1.600 |
R-factor | 0.2014 |
Rwork | 0.201 |
R-free | 0.21620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2h5q |
RMSD bond length | 0.014 |
RMSD bond angle | 1.687 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 67.120 | 67.120 | 1.640 |
High resolution limit [Å] | 1.600 | 7.160 | 1.600 |
Rmerge | 0.066 | 0.025 | 1.223 |
Rmeas | 0.072 | 0.027 | 1.384 |
Total number of observations | 240760 | ||
Number of reflections | 39100 | 478 | 2425 |
<I/σ(I)> | 14.8 | 50.17 | 1.09 |
Completeness [%] | 96.0 | 96.2 | 81.8 |
Redundancy | 6.158 | 6.577 | 4.418 |
CC(1/2) | 0.999 | 0.999 | 0.506 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 291 | PEG 6000, tri-sodium citrate, lithium chloride |