6YK8
OTU-like deubiquitinase from Legionella -Lpg2529
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-12-17 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.070333 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.534, 140.979, 57.437 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.530 - 2.420 |
R-factor | 0.2312 |
Rwork | 0.229 |
R-free | 0.28310 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 0.994 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX (1.17.1_3660) |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.530 | 2.506 |
High resolution limit [Å] | 2.420 | 2.420 |
Rmerge | 0.031 | 0.377 |
Number of reflections | 23185 | 2278 |
<I/σ(I)> | 14.85 | |
Completeness [%] | 99.2 | |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.811 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 25 % PEG3350, 100 mM Tris-HCl pH 8.5, 200 mM NaCl |