6YJD
Lamin A coil2 dimer stabilized by N-terminal capping
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.978565 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 117.250, 117.250, 93.156 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.620 - 2.900 |
Rwork | 0.253 |
R-free | 0.30420 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.761 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | Auto-Rickshaw |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.620 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 8792 | 847 |
<I/σ(I)> | 20.27 | 0.99 |
Completeness [%] | 98.3 | |
Redundancy | 19.2 | |
CC(1/2) | 0.999 | 0.934 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.2 | 277 | 35% (v/v) methanol, 0.2 M MgCl2 and 0.1 M HEPES |