6YHQ

Crystal Structure of Fab F5.18.6, anti-Plasmodium vivax AMA1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Collection date	2005-12-05
Detector	ADSC QUANTUM 4r
Wavelength(s)	0.9330
Spacegroup name	P 21 21 2
Unit cell lengths	95.080, 114.990, 40.680
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.000 - 1.890
R-factor	0.1872
Rwork	0.185
R-free	0.23870
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1clo 1qkz
RMSD bond length	0.008
RMSD bond angle	1.020
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	AMoRE
Refinement software	BUSTER (2.10.3 (3-OCT-2019))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	73.320	1.990
High resolution limit [Å]	1.890	1.890
Rmerge	0.131	0.858
Rmeas	0.142	0.942
Rpim	0.053	0.381
Number of reflections	36659	5255
<I/σ(I)>	9.9	1.9
Completeness [%]	99.9	99.9
Redundancy	7	5.8
CC(1/2)	0.997	0.415

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	290	0.18M KSCN, 16% PEG4000, 0.005M Tris