6YFU

Virus-like particle of Wenzhou levi-like virus 4

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-10-19
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97776
Spacegroup name	I 2 3
Unit cell lengths	551.800, 551.800, 551.800
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.958 - 4.018
R-factor	0.2426
Rwork	0.242
R-free	0.24980
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2ms2
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	FFT
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	49.958	49.958	4.240
High resolution limit [Å]	4.000	11.770	4.000
Rmerge	0.882	0.110	6.402
Rmeas	0.893	0.111	6.482
Total number of observations	9650681
Number of reflections	229056	9293	33519
<I/σ(I)>	5.2	31.41	0.6
Completeness [%]	98.3	98.5	90.1
Redundancy	42.132	40.002	39.967
CC(1/2)	0.994	0.999	0.201

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	293	30 % MPD, 0.1 M MES pH 6.5